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- W2010545946 abstract "Abstract The externally prepared black-coloured copper oxide ( T ⋍ 700 K, P O 2 ⋍ 100 torr) on a Cu(100) surface is identified by electron spectroscopy as CuO. Compared to the red-coloured Cu(I) oxide (in situ oxidation at T ⩾ 400 K, P O 2 ⩽ 0.5 torr, ∼ 10 9 L), the He(I)- excited photoemisson from CuO reveals characteristic shake-up satellites 10–12 eV below E F and a broadened emission from overlapping oxygen-induced 2 p and Cu 3 d states. From the AES and ELS results, in correlation with the data from core electron spectroscopy, chemical shifts of Cu 2 p , Cu 3 s and Cu 3 p in CuO to higher binding energy and decreases in binding energy of the oxygen-induced states were deduced. The unoccupied electron states of Cu at 5 and 7.5 eV above E F — postulated from the ELS results — are preserved in Cu 2 O and CuO compounds. Annealing of the Cu(II) oxide at 670 K is accompanied by decomposition into Cu 2 O due to the solid-state reaction following the scheme: 2CuO → 1/2 O 2 + Cu 2 O." @default.
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- W2010545946 date "1980-01-01" @default.
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- W2010545946 title "Identification of Cu(I) and Cu(II) oxides by electron spectroscopic methods: AES, ELS and UPS investigations" @default.
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- W2010545946 doi "https://doi.org/10.1016/0368-2048(80)80035-1" @default.
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