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- W2010660044 abstract "Two new symmetrical and asymmetrical Zn(II) complexes of a pentadentate (N 5 ) macrocyclic Schiff-base ligands, were prepared via templated [1+1] cyclocondensation of 2,6-diacetylpyridine with two different amines containing piperazine moiety. The complexes have been characterized by variety spectroscopic methods and for asymmetric complex crystal structure was determined by X-ray diffraction. Two symmetrical and asymmetrical Zn(II) complexes of a pentadentate (N 5 ) macrocyclic Schiff-base ligands, were prepared via templated [1 + 1] cyclocondensation of 2,6-diacetylpyridine with two different amines containing piperazine moiety. The complexes have been characterized by a variety of methods including, IR, FAB mass spectrometry, elemental analysis and conductivity measurements. The crystal structure of the asymmetric complex, [ZnL 1 Br]ClO 4 was determined by X-ray diffraction. It is shown that in the solid state the complex adopts a distorted pentagonal–pyramidal geometry, with the macrocycle in the pentagonal plane and the bromide ion in the axial position." @default.
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- W2010660044 date "2009-11-01" @default.
- W2010660044 modified "2023-10-18" @default.
- W2010660044 title "Synthesis and characterization of two zinc(II) macrocyclic Schiff-base complexes containing piperazine moiety, crystal structure of one complex" @default.
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- W2010660044 doi "https://doi.org/10.1016/j.poly.2009.07.012" @default.
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