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- W2010686409 abstract "The evolution of MgAl layered double hydroxides (LDHs), prepared by the sol−gel method, throughout the synthesis−crystallization−calcination−reconstruction process is thoroughly studied and compared to a coprecipitated analogue. X-ray diffraction and transmission electron microscopy provide useful information about crystallinity and morphology of the samples. It was found that crystal sizes do not necessarily decrease after calcination−reconstruction. Furthermore, aluminum coordination is studied by 27Al MAS nuclear magnetic resonance and by X-ray photoelectron spectroscopy (XPS), revealing significant differences in the relative populations of tetrahedral aluminum in the surface and the bulk of the calcined sol−gel LDHs. Magnesium and oxygen structural environments are also studied by XPS. A possible correlation between crystal sizes of calcined LDHs and the amount of O2− surface species is discussed. Differences in the structural environment of magnesium in the as-synthesized and the reconstructed LDH a..." @default.
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- W2010686409 date "2010-01-12" @default.
- W2010686409 modified "2023-10-14" @default.
- W2010686409 title "Comprehending the Thermal Decomposition and Reconstruction Process of Sol−Gel MgAl Layered Double Hydroxides" @default.
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- W2010686409 doi "https://doi.org/10.1021/jp910538r" @default.
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