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- W2010694598 abstract "Starting 1,2,3,4-tetra- O -acetyl-6- O -tosyl-β-D-glucopyranose ( 3 ) was converted into 2,3,4-tri- O -acetyl-1-thio-6- O -tosyl-β-D-glucopyranose ( 6 ) via intermediate glycosyl bromide 4 and S -thiouronium salt 5 . Treatment of compound 6 with sodium methoxide gave 1,6-anhydro-1-thio-β-D-glucopyranose (thiolevoglucosan 2a ). The isomeric sulfoxides 7 and 8 were prepared by selective oxidation of thiolevoglucosan 2a with hydrogen peroxide or 3-chloroperoxybenzoic acid. The structure of new compounds was confirmed by 1 H and 13 C NMR spectroscopy or by X-ray analysis; magnetic anisotropy of the sulfinyl and sulfonyl group has been discussed." @default.
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- W2010694598 date "2006-01-01" @default.
- W2010694598 modified "2023-10-18" @default.
- W2010694598 title "1,6-Anhydro-1-thio-β-D-glucopyranose (Thiolevoglucosan) and the Corresponding Sulfoxides and Sulfone" @default.
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- W2010694598 doi "https://doi.org/10.1135/cccc20060311" @default.
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