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• W2010701680 abstract "A series of [RuX(dioxolene)(terpy)] (terpy = terpyridine; X = Cl, OAc) and one-electron oxidized complexes were prepared. The molecular structures of [RuCl(O2C6H2-3,5-Bu2)(terpy)] (1) and [Ru(OAc)(O2C6H4)(terpy)] (3) were determined by X-ray crystallography. Crystal data for 1: monoclinic, space group P21/c, Z = 8, a = 11.548(1), b = 18.224(5), c = 30.002(8) Å, β = 96.51(2)°, and R = 0.077 (Rw = 0.068). Crystal data for 3: monoclinic, space group C2/c, Z = 8, a = 13.355(5), b = 12.131(4), c = 26.645(4) Å, β = 92.46(2)°, and R = 0.041 (Rw = 0.041). Although the binding mode of O2C6H2-3,5-Bu2 to Ru was not determined by the molecular structure of 1, the carbon–oxygen and carbon–carbon bond lengths of O2C6H4 in 3 were consistent with those of catecholato ligands. Electronic absorption spectra of [RuX(dioxolene)(terpy)] were explained by the electronic structure of [RuIIX(semiquinone)(terpy)] rather than [RuIIIX(catecholato)(terpy)], while the reverse assignment was deduced from the IR spectra. Moreover, ESR spectra showed hyper-fine structures due to the contribution of semiquinone superimposed on an axial pattern of the Ru(III) center, indicating a resonance equilibrium between [RuIIX(semiquinone)(terpy)] and [RuX(dioxolene)(terpy)]." @default.
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• W2010701680 date "1998-04-01" @default.
• W2010701680 modified "2023-10-06" @default.
• W2010701680 title "Synthesis and Characterization of Ruthenium Terpyridine Dioxolene Complexes: Resonance Equilibrium between Ru^III–Catechol and Ru^II–Semiquinone Forms" @default.
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• W2010701680 doi "https://doi.org/10.1246/bcsj.71.867" @default.
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