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- W2010745904 abstract "Two microextraction techniques – liquid phase microextraction based on solidification of a floating organic drop (LPME-SFO) and dispersive liquid–liquid microextraction combined with a solidification of a floating organic drop (DLLME-SFO) – are explored for benzene, toluene, ethylbenzene and o-xylene sampling and preconcentration. The investigation covers the effects of extraction solvent type, extraction and disperser solvents' volume, and the extraction time. For both techniques 1-undecanol containing n-heptane as internal standard was used as an extracting solvent. For DLLME-SFO acetone was used as a disperser solvent. The calibration curves for both techniques and for all the analytes were linear up to 10 μg/mL, correlation coefficients were in the range 0.997–0.998, enrichment factors were from 87 for benzene to 290 for o-xylene, detection limits were from 0.31 and 0.35 μg/L for benzene to 0.15 and 0.10 μg/L for o-xylene for LPME-SFO and DLLME-SFO, respectively. Repeatabilities of the results were acceptable with RSDs up to 12%. Being comparable with LPME-SFO in the analytical characteristics, DLLME-SFO is superior to LPME-SFO in the extraction time. A possibility to apply the proposed techniques for volatile aromatic hydrocarbons determination in tap water and snow was demonstrated." @default.
- W2010745904 created "2016-06-24" @default.
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- W2010745904 date "2009-09-23" @default.
- W2010745904 modified "2023-10-07" @default.
- W2010745904 title "Dispersion-solidification liquid-liquid microextraction for volatile aromatic hydrocarbons determination: Comparison with liquid phase microextraction based on the solidification of a floating drop" @default.
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- W2010745904 doi "https://doi.org/10.1002/jssc.200900360" @default.
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