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- W2010914095 abstract "Abstract The fluoro‐boroarsenate NH 4 [BAsO 4 F] has been obtained by the melt reaction of NH 4 H 2 AsO 4 , B(OH) 3 and LiBF 4 . The dry reaction mixture, in a 3:3:2 ratio, was treated at 240 °C for 14 days. After cooling to room temperature and washing with hot water, the product was isolated as colourless crystals and powder. The crystal structure was determined by single‐crystal X‐ray diffraction. The structure consists of [BAsO 4 F] – layers, separated by ammonium ions, having a unique orientation pattern of the tetrahedra forming the constituent six‐membered rings. The topology of the fluoro‐boroarsenate layer is related to those of the silicate δ‐Na 2 Si 2 O 5 and the borophosphate Mg(H 2 O) 2 [B 2 P 2 O 8 (OH) 2 ]·H 2 O. NH 4 [BAsO 4 F] was further characterised by powder X‐ray diffraction, IR spectroscopy and EDX analyses." @default.
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- W2010914095 date "2009-10-01" @default.
- W2010914095 modified "2023-09-25" @default.
- W2010914095 title "NH4[BAsO4F] - a New Layer Fluoro-boroarsenate with a Silicate Related Topology" @default.
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- W2010914095 doi "https://doi.org/10.1002/zaac.200900183" @default.
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