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- W2011125312 abstract "The effect of flow history, processing temperature, and exit draw ratio have been studied for copolymers of vinylidene fluoride/trifluoroethylene of molar compositions 66/34 and 75/25%. The copolymers were extruded through an impinging channels film die which produces a mixed extension and shearing flow as well as a slit die. Stress fields during flow were measured using flow birefringence. Differential Scanning Calorimetry (DSC) analyses were used to characterize the thermal behavior; and flat film and Wide Angle X-ray Scattering (WAXS) were used to evaluate the crystal structure and morphology of the extrudates. Extensional melt stresses on the order of 6.35 × 105 Pa were necessary to induce sufficient orientation for crystallization of water-cooled 66/34 mol % copolymers into the all-trans configuration. Preorientation of the melt by extensional stresses enhanced the transformation of the 3/1 helical to an all-trans structure in the 66/34 copolymer as well as producing a more compact unit cell in the 75/25 mol % copolymer leading to as much as a 7°C higher Curie transition temperature." @default.
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- W2011125312 date "1991-06-01" @default.
- W2011125312 modified "2023-09-24" @default.
- W2011125312 title "Processing-Property interactions in vinylidene fluoride/trifluoroethylene random copolymers" @default.
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- W2011125312 doi "https://doi.org/10.1002/pen.760311107" @default.
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