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- W2011186836 abstract "The self-assembly of colloidal nanocrystals into ordered superstructures depends critically on the shape of the nanocrystal building blocks. We investigated the self-assembly of cubic PbSe nanocrystals from colloidal suspensions in real-time using in situ synchrotron-based X-ray scattering. We combined small-angle and wide-angle scattering to investigate the translational ordering of nanocrystals and their orientational ordering in the lattice sites, respectively. We found that cubic PbSe nanocrystals assembled into a face-up (i.e., [100] normal to the interface) configuration at the liquid/substrate interface whereas nanocubes at the liquid/air interface assume a corner-up (i.e., [111] normal to the interface) configuration. The latter nanocrystal superlattice displays polymorphism as a function inter-NC separation distance. We explain the observed superlattice structure polymorphs in terms of the interactions directing the self-assembly. Insights into the directed self-assembly of superlattices gained from this study have important implication on the future development of nanocrystals as building blocks in artificial solids." @default.
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- W2011186836 date "2012-08-17" @default.
- W2011186836 modified "2023-09-23" @default.
- W2011186836 title "Interface-Induced Nucleation, Orientational Alignment and Symmetry Transformations in Nanocube Superlattices" @default.
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- W2011186836 doi "https://doi.org/10.1021/nl3026289" @default.
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