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• W2011189332 endingPage "3928" @default.
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• W2011189332 abstract "Abstract The curing kinetics of a novel liquid crystalline epoxy resin with combining biphenyl and aromatic ester‐type mesogenic unit, diglycidyl ether of 4,4′‐bis(4‐hydroxybenzoyloxy)‐3,3′,5,5′‐tetramethyl biphenyl (DGE‐BHBTMBP), and the curing agent diaminodiphenylsulfone (DDS) was studied using the advanced isoconvensional method (AICM). DGE‐BHBTMBP/DDS curing system was investigated the curing behavior by means of differential scanning calorimetry (DSC) during isothermal and nonisothermal processes. Only one exothermal peak appeared in isothermal DSC curves. A variation of the effective activation energy with the extent of conversion was obtained by AICM. Three different curing stages were confirmed. In the initial curing stage, the value of E a is dramatically decreased from ∼90 to ∼20 kJ/mol in the conversion region 0–0.2 for the formation of LC phase. In the middle stage, the value of E a keeps about ∼80 kJ/mol for cooperative effect of reaction mechanism and diffusion control. In the final stage, a significant increase of E a from 84 to 136 kJ/mol could be caused by the mobility of longer polymer chains. © 2007 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 3922–3928, 2007" @default.
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• W2011189332 date "2007-07-18" @default.
• W2011189332 modified "2023-10-14" @default.
• W2011189332 title "Studies on curing kinetics of a novel combined liquid crystalline epoxy containing tetramethylbiphenyl and aromatic ester-type mesogenic group with diaminodiphenylsulfone" @default.
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• W2011189332 doi "https://doi.org/10.1002/pola.22143" @default.
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