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- W2011217085 abstract "Abstract Since known methods for the quantitative determination of free carbon in boron carbide were found to be unsatisfactory, a new method was developed based on a modified Meerson-Samsonov technique, i.e. wet chemical dissolution in hot chromic-sulphuric-iodic acid mixtures. All free carbon, and usually a small amount of combined carbon, is oxidized to carbon dioxide, which is measured coulometrically as a function of the oxidation time. From the CO2 concentration versus time curve plotted, the free carbon content can be calculated; partial oxidation of combined carbon is accounted for by graphical extrapolation. The method was successfully applied also to SiC and further to dense ternary composites made from SiC, boron carbide and carbon. Especially in the case of submicrometre-sized particle carbide powders the new free carbon analyser proved to be very useful." @default.
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- W2011217085 date "1986-03-01" @default.
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- W2011217085 title "A wet chemical method for the determination of free carbon in boron carbide, silicon carbide and mixtures thereof" @default.
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- W2011217085 doi "https://doi.org/10.1016/0022-5088(86)90004-4" @default.
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