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- W2011246992 abstract "Three-dimensional cubic (Im3m) periodic mesoporous organosilicas with aromatic benzene- and thiophene-bridging groups were synthesized using 1,4-bis(triethoxysilyl)benzene and 2,5-bis(triethoxysilyl)thiophene as organosilica precursors in the presence of a F127 PEO–PPO–PEO triblock copolymer under acidic conditions. Highly ordered 3D cubic (Im3m) mesostructure was confirmed by synchrotron small angle X-ray scattering and transmission electron microscopy. Nitrogen adsorption analysis of the aforementioned samples (extracted and additionally calcined in nitrogen at 375–400 °C) revealed their high surface area (460–630 m2 g−1) and accessible ordered large pores (in the range of 6–9 nm). High thermal stability of these benzene- and thiophene-PMO samples (up to 500 and 400 °C, respectively) was confirmed by thermogravimetric analysis, while their framework chemistry was studied by solid-state 13C and 29Si MAS NMR." @default.
- W2011246992 created "2016-06-24" @default.
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- W2011246992 date "2009-01-01" @default.
- W2011246992 modified "2023-10-16" @default.
- W2011246992 title "Three-dimensional cubic (Im3m) periodic mesoporous organosilicas with benzene- and thiophene-bridging groups" @default.
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- W2011246992 doi "https://doi.org/10.1039/b817967k" @default.
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