Matches in SemOpenAlex for { <https://semopenalex.org/work/W2011285167> ?p ?o ?g. }
- W2011285167 endingPage "1063" @default.
- W2011285167 startingPage "1053" @default.
- W2011285167 abstract "The concept of a nonresonant microwave applicator for continuous-flow organic chemistry is introduced and evaluated. The frequency of the incident microwave radiation can be adjusted between 2.4 and 2.5 GHz to optimize the energy absorbance. The temperature of the reaction is monitored by five IR sensors, and their signals can be used to automatically adjust the power output from the microwave generator. The heating of several different solvents up to 20 °C above the standard boiling point has been explored. Several different organic reactions have been successfully carried out using a 200 mm × ⌽ 3 mm tubular borosilicate reactor and a flow between 47 and 2120 μL/min. The microwave heating pattern was visualized with an IR camera. The transformations include palladium-catalyzed coupling reactions (oxidative Heck and Suzuki reactions), heterocyclic chemistry (oxathiazolone and Fischer indole synthesis), rearrangement (Claisen), and a Diels–Alder cycloaddition reaction. A scale-out to 57 mmol/h was performed with the Fischer indole reaction." @default.
- W2011285167 created "2016-06-24" @default.
- W2011285167 creator A5008347976 @default.
- W2011285167 creator A5058891726 @default.
- W2011285167 creator A5059305604 @default.
- W2011285167 creator A5062151428 @default.
- W2011285167 creator A5076252926 @default.
- W2011285167 creator A5089318880 @default.
- W2011285167 date "2012-03-09" @default.
- W2011285167 modified "2023-09-23" @default.
- W2011285167 title "Evaluation of a Nonresonant Microwave Applicator for Continuous-Flow Chemistry Applications" @default.
- W2011285167 cites W1963856269 @default.
- W2011285167 cites W1965219699 @default.
- W2011285167 cites W1973447883 @default.
- W2011285167 cites W1975396841 @default.
- W2011285167 cites W1977202432 @default.
- W2011285167 cites W1978890358 @default.
- W2011285167 cites W1980123294 @default.
- W2011285167 cites W1980803709 @default.
- W2011285167 cites W1981670174 @default.
- W2011285167 cites W1981761223 @default.
- W2011285167 cites W1991667695 @default.
- W2011285167 cites W1992850824 @default.
- W2011285167 cites W1993257128 @default.
- W2011285167 cites W1996958456 @default.
- W2011285167 cites W1997305166 @default.
- W2011285167 cites W2007053762 @default.
- W2011285167 cites W2013760875 @default.
- W2011285167 cites W2017024340 @default.
- W2011285167 cites W2027404044 @default.
- W2011285167 cites W2029193201 @default.
- W2011285167 cites W2029810770 @default.
- W2011285167 cites W2032734313 @default.
- W2011285167 cites W2034137439 @default.
- W2011285167 cites W2040941091 @default.
- W2011285167 cites W2042544912 @default.
- W2011285167 cites W2044803938 @default.
- W2011285167 cites W2048269143 @default.
- W2011285167 cites W2048974066 @default.
- W2011285167 cites W2051709026 @default.
- W2011285167 cites W2061343703 @default.
- W2011285167 cites W2064737932 @default.
- W2011285167 cites W2065274980 @default.
- W2011285167 cites W2065518405 @default.
- W2011285167 cites W2065649191 @default.
- W2011285167 cites W2066558102 @default.
- W2011285167 cites W2071810694 @default.
- W2011285167 cites W2076064777 @default.
- W2011285167 cites W2076883432 @default.
- W2011285167 cites W2080168485 @default.
- W2011285167 cites W2086156805 @default.
- W2011285167 cites W2087659295 @default.
- W2011285167 cites W2090081862 @default.
- W2011285167 cites W2093161659 @default.
- W2011285167 cites W2095573393 @default.
- W2011285167 cites W2105677452 @default.
- W2011285167 cites W2108647642 @default.
- W2011285167 cites W2117573771 @default.
- W2011285167 cites W2123021412 @default.
- W2011285167 cites W2135213872 @default.
- W2011285167 cites W2137322651 @default.
- W2011285167 cites W2157572033 @default.
- W2011285167 cites W2161205795 @default.
- W2011285167 cites W2163322780 @default.
- W2011285167 cites W2167199452 @default.
- W2011285167 cites W2169315779 @default.
- W2011285167 cites W2172558013 @default.
- W2011285167 cites W2318169400 @default.
- W2011285167 cites W2950028905 @default.
- W2011285167 cites W2951061630 @default.
- W2011285167 cites W2951516299 @default.
- W2011285167 cites W2951835302 @default.
- W2011285167 cites W2952139546 @default.
- W2011285167 cites W2953129060 @default.
- W2011285167 cites W4211139985 @default.
- W2011285167 cites W4230346864 @default.
- W2011285167 cites W4232374969 @default.
- W2011285167 cites W4234882500 @default.
- W2011285167 cites W4256368448 @default.
- W2011285167 doi "https://doi.org/10.1021/op300003b" @default.
- W2011285167 hasPublicationYear "2012" @default.
- W2011285167 type Work @default.
- W2011285167 sameAs 2011285167 @default.
- W2011285167 citedByCount "61" @default.
- W2011285167 countsByYear W20112851672012 @default.
- W2011285167 countsByYear W20112851672013 @default.
- W2011285167 countsByYear W20112851672014 @default.
- W2011285167 countsByYear W20112851672015 @default.
- W2011285167 countsByYear W20112851672016 @default.
- W2011285167 countsByYear W20112851672017 @default.
- W2011285167 countsByYear W20112851672018 @default.
- W2011285167 countsByYear W20112851672019 @default.
- W2011285167 countsByYear W20112851672020 @default.
- W2011285167 countsByYear W20112851672021 @default.
- W2011285167 countsByYear W20112851672022 @default.
- W2011285167 countsByYear W20112851672023 @default.
- W2011285167 crossrefType "journal-article" @default.
- W2011285167 hasAuthorship W2011285167A5008347976 @default.