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• W2011304292 abstract "Monoclinic ferrous tungstate (FeWO4) microcrystals with hierarchical nano/microstructures have been selectively synthesized via a facile hydrothermal process in the presence of ethylenediamine tetraacetic acid disodium salt (Na2EDTA) and hexamethylenetetramine (HMT). HMT played triple roles as the reducing agent, alkaline source, and crystal growth modifier, while Na2EDTA served as the chelating reagent and structure-directing agent. The appropriate conditions for synthesis of multilayer flower-like FeWO4 were 200 °C and 8 h with the concentrations of Na2EDTA and HMT at 0.03 mol L−1 and 0.025 mol L−1, respectively. The morphology of FeWO4 showed dramatic changes from a bulky amorphous crystal to multilayer hexangular microcrystals with increasing Na2EDTA concentration, while increasing HMT concentration would transform the hexagonal structure to a sixfold symmetry architecture and the aspect ratio of symmetry axis decreased gradually. Ostwald ripening and the self-assembled process was proposed for the possible formation mechanism. The photoluminescence (PL) intensity of the multilayer FeWO4 microcrystals was higher than that of other FeWO4 structures. Magnetic measurement of hexangular FeWO4 microcrystals showed a small ferromagnetic ordering at low temperature. Furthermore, this work may open novel routes to the chelating reagent-assisted synthesis of hierarchical architectures with various morphologies." @default.
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• W2011304292 date "2011-01-01" @default.
• W2011304292 modified "2023-10-14" @default.
• W2011304292 title "Controlled synthesis, growth mechanism and optical properties of FeWO4 hierarchical microstructures" @default.
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• W2011304292 doi "https://doi.org/10.1039/c1ce05416c" @default.
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