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- W2011305963 abstract "Rapid microwave-assisted solution-phase peptide synthesis protocol has been developed. The reaction temperature of 50 °C, 40 W and short coupling time of 28 min gave racemization-free synthesis of peptides in 50–80% yield. The method is applicable with equal ease in coupling both side-chain protected and unprotected amino acids indicating reactive-functional group tolerance and high atom-economy. In the case of dipeptides, DIC/HONB-mediated coupling rendered the best results. In the case of tri- and tetrapeptides, HATU/HOAt/DIEA emerged as the best coupling combination." @default.
- W2011305963 created "2016-06-24" @default.
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- W2011305963 date "2012-12-01" @default.
- W2011305963 modified "2023-09-30" @default.
- W2011305963 title "Rapid microwave-assisted solution-phase peptide synthesis" @default.
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- W2011305963 doi "https://doi.org/10.1016/j.tetlet.2012.10.028" @default.
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