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- W2011381845 abstract "The reaction of (1,4,7-triazaheptane)Cu(NO3)2 with 2-amino-5-methyl-1,3-thiazole (amtz) yields the compound [(amtz)(dien)Cu](NO3)2 (dien=1,4,7-triazaheptane). The compound has been characterised by elemental analyses, molar conductance and magnetic measurements, as well as by its electronic and IR spectra and X-ray diffraction. There are two crystallographically discernible cations [(amtz)(dien)Cu]2+ and four NO3− in the asymmetric unit of the structure. Dien is tridentate with mean Cu–N=1.997(5) and 2.021(5) Å in the two Cu-ions, respectively. Amtz is coordinated through its endocyclic N with Cu–N=2.063(7) and 1.945(6) Å in the two ions, respectively. The CuN4 unit is approximately square planar and almost perpendicular to the tz plane. Both the cations make two long (trans-Cu…O=2.6–2.7 Å) contacts. Ab initio calculations on the constituent fragments [(dien)Cu]2+, [(amtz)Cu]2+ and [(dien)(amtz)Cu]2+ reproduced the average molecular structure parameters of the two Cu-ions in the unit cell and also helped interpret the details of the molecular structure as well as the assignment of the vibrational and electronic spectra." @default.
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- W2011381845 date "1999-04-01" @default.
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- W2011381845 title "Crystal and molecular structures of [(2-amino-5-methyl-1,3-thiazole)(1,4,7-triazaheptane)copper(II)] dinitrate" @default.
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- W2011381845 doi "https://doi.org/10.1016/s0277-5387(99)00048-0" @default.
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