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- W2011472039 abstract "Die Darstellung der Cyclopentadienyl-vanadium(V)-Verbindungen tC4H9NVCpX2 (X=SR, SeC6H5, Br, I), tC4H9NVCp(StC4H9) und tC4H9NVCp[s(CH2)3S] (4) wird beschrieben; als Ausgangsverbindung wird tC4H9NVCpCI2 eingesetzt. tC4H9NVCl3 reagiert mit BBr3 und Bl3 unter Halogenaustausch und Bildung der Trihalogenide tC4H9NVX3 (X=Br, I). Alle dargestellten Verbindungen werden 1H- und 51V-NMR-spektroskopisch charakterisiert. Die Röntgenstrukturanalyse von 4 zeigt das Vanadiumatom in einer verzerrt tetraedrischen Anordnung der Liganden; der VS2C3-Ring liegt in der Sesselkonformation vor. Synthesis and NMR Spectroscopic Studies of tert-Butylimino-cyclopentadienylvanadium(V) Compounds tC4H9NVCpX2 (X=SR, SeC6H5, Br, I) Syntheses of the cyclopentadienylvanadium(V) compounds tC4H9NVCpX2 (X=SR, SeC6H5, Br, I) tC4H9NVCp (StC4H9) and tC4H9NVCp[S(CH2)3S] (4) are described starting from tC4H9NVCpCl2. tC4H9NVCl3 reacts with BBr3 and BI3 by halogen exchange forming the trihalogenides tC4H9NVX3 (X=Br, I). All compounds obtained are characterized by 1H and 51V NMR spectroscopy. 4 has been found by X-ray diffraction analysis to be a distorted tetrahedral vanadium complex with a chair conformation of the VS2C3-ring." @default.
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- W2011472039 date "1992-03-01" @default.
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- W2011472039 title "Darstellung und NMR-spektroskopische Untersuchungen der tert-Butylimino-cyclopentadienylvanadium (V)-VerbindungentC4H9N?VCpX2 (X=SR, SeC6H5, Br, I)" @default.
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- W2011472039 doi "https://doi.org/10.1002/zaac.19926090308" @default.
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