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• W2011497166 abstract "Synthesis and spectroscopic characterisation of tetrabutylammonium salts of heteropolyanions (NBu4HPAS) of Keggin’s (NBu4)5H2PW11O39, (NBu4)6HPMo2W9O39, (NBu4)6H2SiMo2W9O39, (NBu4)4H3PMo2W9O39, (NBu4)6HPMo2W9O39, Dawson’s type (NBu4)9HP2W17O61 and Preyssler heteropolyanion (NBu4)12[(Eu)P5W30O110] are presented. Extraction procedure has been selected as the best method for synthesis of compositions containing an organic counter anion. Elemental and thermogravimetric analysis, spectrophotometric determination of W and Mo, and FTIR spectra have been applied for analysis of the compositions obtained. The complexation studies were carried out with the use of Nd(III) and Er(III) absorption spectra (in the range of their hypersensitive transitions) and Eu(III) luminescence lifetime measurements. Threshold bootstrap computer-assisted target factor analysis (TB CAT) has been applied to evaluate the Nd(III) and Er(III) spectra in DMF and DMSO solutions and to estimate conditional formation constants for Ln(III)(NBu4HPAS)2 sandwich species (Ln(III)Nd(III), Er(III)). Luminescence characterisation of the NBu4EuHPAS compounds concerning their intensity, quantum yield and luminescence lifetime of Eu(III) ion in non-aqueous solutions and solid are discussed." @default.
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• W2011497166 date "2004-07-01" @default.
• W2011497166 modified "2023-10-17" @default.
• W2011497166 title "Synthesis and spectroscopic characterisation of chosen heteropolyanions and their Ln(III) complexes containing tetrabutylammonium counter ion" @default.
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• W2011497166 doi "https://doi.org/10.1016/j.jallcom.2003.11.126" @default.
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