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• W2011575497 abstract "The low-temperature interaction (up to 550°C) of a pre-reduced palladium modifier with sodium sulfate and sodium selenite on the pyrolytic graphite platform was studied using X-ray photoelectron spectroscopy (XPS) and electron microprobe analysis. The equipment applied allowed the introduction of samples heated in an argon flow into the analytical chamber of the XPS spectrometer without contact with the air. Electron microprobe analysis showed that palladium and sulfur preferably occupy different areas on the platform surface. On the contrary, selenium from sodium selenite tends to occupy areas of the graphite surface covered with palladium. The most probable reason for this is the chemisorption of selenium (IV) on the palladium surface at the drying stage. No changes in the XPS spectra of metallic Pd and S6+ were observed when Na2SO4 and Pd were heated together on the graphite platform in the range 100–550°C. The reduction of sodium selenite on the graphite surface already starts during drying. Pre-reduced palladium intensifies this process. The rate of the reduction is proportional to the amount of palladium, and in the presence of palladium at an atomic ratio of Pd/Se=7.5, the transformation of Se4+ into Se0 completes at 250°C." @default.
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• W2011575497 date "2001-08-01" @default.
• W2011575497 modified "2023-10-13" @default.
• W2011575497 title "Low-temperature transformations of sodium sulfate and sodium selenite in the presence of pre-reduced palladium modifier in graphite furnaces for electrothermal atomic absorption spectrometry" @default.
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• W2011575497 doi "https://doi.org/10.1016/s0584-8547(01)00251-8" @default.
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