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- W2011750474 abstract "A new potential‐step method was used to determine oxygen coverage on platinum, gold, and rhodium. The procedure was based, in part, on the use of an electronic coulometer. Experimental evaluation of the coverage and its theoretical interpretation was obtained by the use of the potential‐step method in conjunction with the potential‐sweep method. The advantage of the step method over the potential‐sweep method for evaluating the degree of coverage is that the step method gives invariant results regardless of whether the technique is anodic or cathodic. The pH was found to have profound effects on the oxygen coverage. In general, changing the pH alters the degree of coverage by oxygen‐containing species probably including carbon dioxide. Changes produced by pH alteration in the potential‐sweep patterns of noble metals may be ascribed in part to the adsorption of carbonaceous impurities and to the pH‐activated amphoteric character of the surface oxides. The oxygen coverage on platinum, a linear function of potential above 0.8V, may be explained in terms of platinum oxide dipoles." @default.
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- W2011750474 date "1970-01-01" @default.
- W2011750474 modified "2023-09-27" @default.
- W2011750474 title "Use of the Potential-Step Method to Measure Surface Oxides" @default.
- W2011750474 doi "https://doi.org/10.1149/1.2407359" @default.
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