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- W2011938645 abstract "Taguchi method is widely used by the engineers and researchers across the globe for optimization of process parameters in view of cost, economy and time. Ultrasound based sonication process was used for deriving the nano-crystals of sirolimus in a narrow range. Seven critical process parameters with three levels were optimized with L18 array design. Crystal size analysis with its zeta potential measured and found that the crystals derived are stable in nature. Also SEM analysis carried out to know size and shape of the crystals and found that the crystals obtained are spherical in nature. Purity of the crystals derived checked with the help of melting point, TLC and HPLC procedures. Characterization of nano-crystals made with Fourier transform infrared spectroscopy and X-ray diffraction analysis. Correlation between the zeta potential and crystal size has been established with the help of scientific and statistical methods. Detailed statistical analysis such as t -test, regression and descriptive statistics of the results has been carried out to explore further information and interactions of process parameters. (© 2012 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim)" @default.
- W2011938645 created "2016-06-24" @default.
- W2011938645 creator A5016047941 @default.
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- W2011938645 date "2011-10-27" @default.
- W2011938645 modified "2023-10-16" @default.
- W2011938645 title "Optimization of process parameters by Taguchi robust design method for the development of nano-crystals of sirolimus using sonication based crystallization" @default.
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- W2011938645 doi "https://doi.org/10.1002/crat.201100329" @default.
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