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- W2012026417 abstract "The feasibility of controlling the transport mechanism of the oxidizing species at the working electrode during the stripping step of potentiometric stripping analysis is demonstrated. When linear diffusion of the oxidizing species is the rate-determining mechanism at the working electrode/solution interface and when the physical properties of the medium are considered to lower the diffusion coefficient of the oxidizing species, the relative sensitivity of the technique is enhanced by a factor of 50 for all the common ions studied by potentiometric stripping analysis. Examples and comparison with the normal procedure are given for Cu, Cd, Zn, Pb, Bi, Tl and Ga. The “stationary electrode” procedure is compatible with the normal instrumentation without great modification; it is self-optimizing with respect to time and resolution and preserves all the inherent advantages of potentiometric stripping analysis compared to other electrochemical techniques of trace analysis. The enhancement of the relative sensitivity by this modification permits measurements in the 0.01–0.1 ppb range for metal ions; the total time required is 2–4 min for a single determination and the relative standard deviations are about 3%." @default.
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- W2012026417 title "Potentiometric stripping analysis at a stationary electrode" @default.
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