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- W2012028222 abstract "Die 1H-NMR-Spektren der vier Triäthylhalogensilane (C2H5)3SiX (X F, Cl, Br, I) und des Triäthylsilans (X H) wurden aufgenommen und ausgewertet. Die Spektren der Verbindungen mit X Cl, Br, I stellen wegen der geringen Differenzen der Chemischen Verschiebung von Methyl- und Methylenprotonen jeweils stark kontrahierte A3B2-Multipletts dar, die bei den Verbindungen mit X H, F durch die zusätzliche Wechselwirkung dieser Atomkerne mit den Methylenprotonen zu (A3B2)3X-Systemen erweitert sind. Die erhaltenen und durch Computerberechnungen gesicherten Werte der Chemischen Verschiebung und der Kopplungskonstanten werden vergleichend diskutiert. PMR spectra of the four triethylhalosilanes (C2H5)3SiX (X F, Cl, Br, I) and of triethylsilane (X H) were recorded and assigned. In the cases of X Cl, Br the spectra are characterized by collapsed A3B2-multiplets, due to small differences in magnetic shielding of methyl and methylene protons. For X H, F these multiplets are extended to (A3B2)3X systems by spin-spin interactions of these nuclei with the methylene protons. Triethyliodosilane shows only a singulet signal for all ethyl hydrogen atoms. The results, being confirmed by theoretically computed spectra, are subjected to a short comparative discussion." @default.
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- W2012028222 date "1964-12-01" @default.
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- W2012028222 title "Die NMR-spektren der triäthylhalogensilane und des triäthylsilans" @default.
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- W2012028222 doi "https://doi.org/10.1016/s0022-328x(00)83262-3" @default.
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