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- W2012029477 abstract "The synthesis of a series of p-bromo-3-N-alkyl spiperone analogues is described. N-alkylation was achieved via reaction of the potassium salt of the spiperone lactam ring with alkyl iodide; subsequent reactions with elemental bromine gave the p-brominated isomers. Optimization studies using no-carrier-added (n.c.a.) 77Br− indicated that radiobromination of N-alkyl spiperone analogues occurs with higher yields and in shorter reaction times when dichloramine-T (DCT) is used rather than H2O2/acetic acid as an oxidant. The production of the title compounds in high effective specific activity with radiochemical yields of 20–30 % using n.c.a. 77Br− and DCT is reported." @default.
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- W2012029477 date "1985-10-01" @default.
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- W2012029477 title "Synthesis of no-carrier-added radiobrominated N-alkylated analogues of spiperone" @default.
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- W2012029477 doi "https://doi.org/10.1002/jlcr.2580221004" @default.
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