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- W2012034811 abstract "Abstract The synthesis and characterization of biscopper(II) complexes of the octaaza ligands 5,5-bis(4′-amino- 2′-azabutyl)-l.9-diamino-3,7-diazanonane (tabm) and 6,6-bis(5 ′-amino-2′-azapentyl)-1,11-diamino-4,8-diazaundecane (tapm) is described. The structure of one of the complexes, Cu2(tabm)(NO3)4·6H20, has been determined by single crystal X-ray diffraction techniques - (R = 0.079), space group P21/a, with a = 12.656(3), b= 15.411(6), c= 16.426(5) A and Z= 4. The copper(II) ions adopt a tetragonally distorted octahedral geometry with the O-Cu-O axes nearly perpendicular. For the Cu2(tapm)(NO3)4 analogue a structure is proposed in which a non-orthogonal arrangement of the O-Cu-O axes is possible. The ESR spectrum (77 K, DMF) of both complexes is discussed and related to the observed and proposed structures and the observed magnetic susceptibilities (μeff = 1.8−1.9,298 K)." @default.
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- W2012034811 date "1986-06-01" @default.
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- W2012034811 title "Bis-copper(II) complexes of binucleating linear octaaza ligands" @default.
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