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- W2012040632 abstract "Abstract A novel method to synthesize GaN crystals was studied by the reaction of Ga with Li 3 N under NH 3 atmosphere. We have already reported the synthesis technique of GaN by the reaction of Ga 2 O 3 with Li 3 N. However, the size of GaN crystals obtained by this method was limited to be smaller than several micrometers because of the solid phase reaction. In order to increase the size of GaN crystals, the method using liquid Ga as gallium source was studied for solid–liquid phase reaction. We found that the GaN crystals with the size of more than 100 μm were synthesized at 750 °C for 24 h under NH 3 atmosphere. We propose the possible reaction mechanism as follows. Lithium amide (LiNH 2 ) is synthesized by the reaction of Li 3 N with NH 3 gas and then the crystal growth of GaN occurs by the reaction of Ga with LiNH 2 . We found that LiNH 2 is a useful nitrogen source for the GaN synthesis method." @default.
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- W2012040632 date "2009-05-01" @default.
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- W2012040632 title "Synthesis of GaN crystal by the reaction of Ga with Li3N in NH3 atmosphere" @default.
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- W2012040632 doi "https://doi.org/10.1016/j.jcrysgro.2009.01.074" @default.
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