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- W2012041575 abstract "The novel quinoxaline substituted (E,E)-dioxime (H2L) containing a hexaoxadiaza macrobicycle [2.2.2B] has been synthesized from the reaction of 4,7,13,16,21,24-hexaoxa-5,6-(2′,3′-diaminobenzo)-1,10-diazabicyclo[8.8.8]hexacosane (4) prepared from 4,7,13,16,21,24-hexaoxa-5,6-(2′,3′-dinitrobenzo)-1,10-diazabicyclo[8.8.8]hexacosane (3) and cyanogendi-N-oxide (5). Only the mononuclear nickel(II) complex with a metal∶ligand ratio of 1∶2 was prepared. This hydrogen-bridged complex was converted into its BF2+ capped analogue by reaction with BF3·Et2O. The reaction of the BF2+ bridged complex with KPF6 gave a heterotrinuclear complex. Structures for the dioxime and its complexes are proposed in accordance with elemental analysis, 1H and 13C NMR, IR and MS spectral data." @default.
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- W2012041575 date "2003-01-01" @default.
- W2012041575 modified "2023-10-17" @default.
- W2012041575 title "The synthesis and characterization of a new (E,E)-dioxime and its homo- and heterotrinuclear complexes containing a hexaoxadiaza macrobicycle moiety" @default.
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- W2012041575 doi "https://doi.org/10.1039/b207693b" @default.
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