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• W2012043961 abstract "This paper is a review of our work on nanocrystalline semiconductor films which exhibit pronounced size quantization effects in three dimensions, manifested by large blue-shifts in their optical absorption spectra. The films are prepared by either chemical solution deposition (CdSe and PbSe) or by electrodeposition from nonaqueous electrolytes (CdSe and CdS). Except for PbSe, where the nanocrystals are surrounded by a matrix, the films are comprised of aggregated nanocrystals. Crystal size (typically from <4 nm to >6 nm), and therefore absorption spectra, can be controlled by deposition temperature, illumination during deposition (for chemically deposited films), solution composition, and post annealing. The crystal size dependence of chemically-deposited films on experimental parameters (temperature, illumination, reactant concentrations) is discussed. CdSe nanocrystals were epitaxially electrodeposited on single-crystal Au. The nanocrystal distribution (isolated or aggregated) could be controlled by deposition current and temperature. All these films exhibit photoelectrochemical behavior but no corresponding solid state photovoltaic behavior. A model is proposed based on electron/hole separation by kinetic differences in charge injection into an electrolyte rather than by a built-in space charge layer in the semiconductor. The films can behave as both ‘n’ - or ‘p’-type, with respect to direction of photocurrent flow, by changes in the semiconductor surface properties and/or the electrolyte, in agreement with this model." @default.
• W2012043961 created "2016-06-24" @default.
• W2012043961 creator A5061755535 @default.
• W2012043961 date "1993-01-01" @default.
• W2012043961 modified "2023-09-26" @default.
• W2012043961 title "Size-Quantized Nanocrystalline Semiconductor Films" @default.
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• W2012043961 doi "https://doi.org/10.1002/ijch.199300015" @default.
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