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• W2012044142 abstract "In this study, headspace single drop microextraction (HS-SDME) method in combination with electrothermal atomic absorption spectrometry (ETAAS) method was developed and validated for the speciation and determination of inorganic mercury (iHg) and methylmercury (MeHg). MeHg and iHg species were reduced to volatile methylmercury hydride (CH3HgH) and elemental mercury, respectively, in the presence of NaBH4 and trapped onto a drop of acceptor phase in the tip of a microsyringe. Thiourea and ammonium pyrrolydinedithiocarbamate (APDC) were tested as the acceptor phase. The experimental parameters of the method such as microextraction time, temperature, NaBH4 concentration, acceptor phase concentration, and pH of the medium were investigated to obtain distinctive conditions for mercury species. Possible interference effects have also been investigated. In order to validation of the method, analytical figures of merits such as accuracy, precision, limit of detection (LOD), limit of quantitation (LOQ), and linear working range have been evaluated. Accuracy of the method has been verified by analyzing certified reference materials (BCR 453 Tuna fish) and spiked samples. The proposed method was applied for the speciation and determination of mercury species in water and fish samples. Mercury species (MeHg and iHg) have been determined in the real samples with a relative error less than 10%." @default.
• W2012044142 created "2016-06-24" @default.
• W2012044142 creator A5009993165 @default.
• W2012044142 creator A5039132658 @default.
• W2012044142 date "2012-03-02" @default.
• W2012044142 modified "2023-09-25" @default.
• W2012044142 title "Speciation and Determination of Inorganic Mercury and Methylmercury by Headspace Single Drop Microextraction and Electrothermal Atomic Absorption Spectrometry in Water and Fish" @default.
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• W2012044142 doi "https://doi.org/10.1002/clen.201100535" @default.
• W2012044142 hasPublicationYear "2012" @default.
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