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• W2012072004 abstract "Single phase yttrium orthoferrite (YFeO3) nanocrystals have been one-step synthesized by a sol–gel auto-combustion method using nitrates of iron and yttrium as raw materials, citrate acid (CA) and ethylene glycol (EG) as chelating agents and nitrate ammonium as oxidant. The effects of CA/M and the pH value of the solutions on the concentrations of yttrium– and iron–citrate complex species were quantitatively studied to ensure the formation of chemically homogenous gels. The auto-combustion of the dried gels and the microstructural features and magnetic properties of as-synthesized YFeO3 nanocrystals were characterized and investigated by using XRD, FT-IR, TG-DTA, FESEM and VSM. It has been shown that a hexagonal YFeO3 can be formed during the auto-combustion of gels with CA/M = 1.5, EG/CA = 1.5, pH = 6.0 and Q = 35%, the molar ratio of the oxygen available from nitrates (NO3−) to the oxygen required for complete oxidation of fuels to CO2, H2O and N2, while single phase orthorhombic YFeO3 nanocrystals of ∼90 nm in average diameter may be one-step synthesized from the gels with Q = 80%, and show an enhanced weak ferromagnetism characterized with a RT magnetization of 0.45 emu g−1 at the magnetic field 0.35T, a paramagnetism with the susceptibility χ = 2.27 × 10−5 emu g−1 Oe−1, and an extremely low coercive field of 245 Oe." @default.
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• W2012072004 date "2013-01-01" @default.
• W2012072004 modified "2023-10-17" @default.
• W2012072004 title "One-step synthesis of yttrium orthoferrite nanocrystals via sol–gel auto-combustion and their structural and magnetic characteristics" @default.
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• W2012072004 doi "https://doi.org/10.1016/j.matchemphys.2012.10.029" @default.
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