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• W2012074444 abstract "Abstract The reactions of a variety of primary and secondary amines and secondary phosphanes with “GaI” have been examined. In all cases disproportionation reactions occurred which led to the gallium( II ) iodide complexes [Ga 2 I 4 (L) 2 ] [L = NCyH 2 , N t BuH 2 , NCy 2 H, PCy 2 H or P t Bu 2 H (Cy = cyclohexyl)]. All complexes have been crystallographically characterised and have been shown to be dimers possessing Ga−Ga bonds. The reaction of the sterically hindered N‐heterocyclic carbene IPr [ : CN(Ar)C 2 H 2 N(Ar) (Ar = C 6 H 3 i Pr 2 ‐2,6)] with “GaI” was also carried out and the novel salt [Ga 2 I 5 (IPr)][IPrH] was formed in good yield and crystallographically characterised. Finally, the related reaction of the less hindered cyclic carbene IMe [ : CN(Me)C 2 Me 2 N(Me)] with InCl gave a low yield of the crystallographically characterised salt [{InCl(IMe)} 2 (μ‐Cl)(μ‐O)][Cl] which presumably forms due to the presence of adventitious oxygen in the reaction mixture. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2003)" @default.
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• W2012074444 date "2003-06-24" @default.
• W2012074444 modified "2023-10-18" @default.
• W2012074444 title "The Reactivity of Primary and Secondary Amines, Secondary Phosphanes and N‐Heterocyclic Carbenes towards Group‐13 Metal(<scp>I</scp>) Halides" @default.
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• W2012074444 doi "https://doi.org/10.1002/ejic.200300068" @default.
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