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• W2012078202 abstract "Abstract The applicability of size-exclusion chromatography (SEC) with on-line inductively coupled plasma-atomic emission spectrometric (ICP-AES) detection for the determination of nickel and vanadium compounds in oil samples was examined. Four mobile phases, tetrahydrofuran, chloroform, xylene and xylene-methanol, in combination with two stationary phases, a polystyrene-divinylbenzene and a silica-based diol column packing, were characterized with regard to the shapes of the nickel and vanadium elution profiles and overall recoveries. Tetrahydrofuran and chloroform could successfully be introduced into the ICP at conventional flow-rates by the application of an aerosol cooling setup in the SEC-ICP interface. The recoveries on the diol-modified silica gel packing were significantly smaller than those found with the polystyrene-divinylbenzene packing. With tetrahydrofuran and xylene-methanol nearly complete recoveries and similar elution profiles were obtained with the polystyrene-divinylbenzene packing, whereas for chloroform and xylene adsorption of high-molecular-weight components hampered the interpretation." @default.
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• W2012078202 date "1989-01-01" @default.
• W2012078202 modified "2023-09-25" @default.
• W2012078202 title "Selection of conditions for the molecular size speciation of vanadium and nickel complexes in oil by size-exclusion chromatography coupled with inductively coupled plasma-atomic emission spectrometry" @default.
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• W2012078202 doi "https://doi.org/10.1016/s0021-9673(00)91341-4" @default.
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