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- W2012093054 abstract "1-Nitropyrene-d9, 1,3-dinitropyrene-d8, 1,6-dinitropyrene-d8, and 1,8-dinitropyrene-d8, used as internal standards for the determination of nitropolycyclic aromatic hydrocarbons (NPAH) in simple and complex mixtures, and required for GC/MS measurements used in the certification of NBS Standard Reference Material (SRM) 1596 (a mixture of nitropyrenes), were synthesized in one step from commercially available pyrene-d10 and nitric acid-d1. The electron impact mass spectra and isotopic purity of 1-nitropyrene-d9 and the deuterated dinitropyrenes were determined; the compounds were characterized by gas chromatpgraphy-mass spectrometry (GC-MS) and by high performance liquid chromatography (HPLC)." @default.
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- W2012093054 date "1989-02-01" @default.
- W2012093054 modified "2023-09-23" @default.
- W2012093054 title "Facile synthesis of 1-nitropyrene-d9 of high isotopic purity" @default.
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- W2012093054 doi "https://doi.org/10.1002/jlcr.2580270203" @default.
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