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- W2012097680 abstract "Abstract The precipitation of calcium oxalate during the titration of acidified solutions of calcium nitrate with potassium oxalate was studied in the temperature range 13–69°C by monitoring changes in pH with time. A critical supersaturation ratio of 30 for incipient precipitation of the solid phase at 25°C was measured that proved to be independent of the titration speed or initial calcium concentration. With increasing temperature this critical supersaturation is observed to decrease. An analysis of the observed change in supersaturation with titration time at relatively high supersaturation, but under conditions where three-dimensional nucleation is not possible, indicates that the rate of growth of the precipitated phase, calcium oxalate monohydrate, varies with the relative supersaturation raised to the power 3.4. This empirical result is different from the observed parabolic rate law in seeded growth experiments and can be explained by a layer-by-layer growth mechanism based on a polynuclear, surface nucleation model." @default.
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- W2012097680 date "1986-09-01" @default.
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- W2012097680 title "Precipitation of calcium oxalate hydrate by titration of acidified calcium nitrate solutions with potassium oxalate" @default.
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- W2012097680 doi "https://doi.org/10.1016/0166-6622(86)80225-6" @default.
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