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- W2012099618 abstract "A porous glass sheet was used as a stationary phase for the thin-layer chromatography (TLC) of inorganic cations. Some cations gave rise to fluorescent compounds when spots on the sheet were heated for detection. The fluorescent cations were screened from commercially available reagents by heating at various temperatures from 100 to 700°C for 15 min. The fluorescent cations foud were Mg, Al, Ca, V, Cu, Zn, Ge, Y, Zr, Mo, Ag, Cd, In, La, Ce, Eu, Tb, Tl, Pb and Bi. Detection limits of lead, vanadium and tin were 300 pmol and that of copper was 3 pmol. Their fluorescence spectra were measured in situ on the sheet and showed hitherto unknown fluorescent reactions. After the separation, the fluorescent spots were overlapped with the triplicate spots detected with 8-hydroxyquinoline or dithizone, which meant that the fluorescent compounds were not due to impurities." @default.
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- W2012099618 date "1992-06-01" @default.
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- W2012099618 title "Fluorescence reactions of inorganic cations heated on a porous glass sheet for thin-layer chromatography" @default.
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- W2012099618 doi "https://doi.org/10.1016/0021-9673(92)85364-y" @default.
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