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• W2012122902 endingPage "4550" @default.
• W2012122902 startingPage "4541" @default.
• W2012122902 abstract "This paper describes a pulsed galvanostatic technique to interrogate ion-selective electrodes (ISEs) with no intrinsic ion-exchange properties. Each applied current pulse is followed by a longer baseline potential pulse to regenerate the phase boundary region of the ion-selective membrane. The applied current fully controls the magnitude and sign of the ion flux into the membrane, thus offering instrumental control over an effect that has become very important in ion-selective electrode research in recent years. The resulting chronopotentiometric response curves essentially mimic traditional ISE behavior, with apparently Nernstian response slopes and selectivities that can be described with the Nicolsky equation. Additionally, the magnitude and sign of the current pulse may be used to tune sensor selectivity. Perhaps most important, however, appears to be the finding that the extent of concentration polarization near the membrane surface can be accurately controlled by this technique. A growing number of potentiometric techniques are starting to make use of nonequilibrium principles, and the method introduced here may prove to be very useful to advance these areas of research. The basic characteristics of this pulsed galvanostatic technique are here evaluated with plasticized poly(vinyl chloride) membranes containing the sodium-selective ionophore tert-butyl calix[4]arene tetramethyl ester and a lipophilic inert salt." @default.
• W2012122902 created "2016-06-24" @default.
• W2012122902 creator A5002989149 @default.
• W2012122902 creator A5016418669 @default.
• W2012122902 date "2003-07-16" @default.
• W2012122902 modified "2023-09-26" @default.
• W2012122902 title "Pulsed Galvanostatic Control of Ionophore-Based Polymeric Ion Sensors" @default.
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• W2012122902 doi "https://doi.org/10.1021/ac034409t" @default.
• W2012122902 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/14632062" @default.
• W2012122902 hasPublicationYear "2003" @default.
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