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• W2012130177 abstract "The polycondensation reaction of 3,4-ethylenedioxythiophene with 2,7-dibromo-9,9-dioctylfluorene via Pd-catalyzed direct arylation gives poly[(3,4-ethylenedioxythiophene-2,5-diyl)-(9,9-dioctylfluorene-2,7-diyl)]. The reaction conditions are optimized in terms of the Pd precatalysts, reaction time, and carboxylic acid additives. The combination of 1 mol% Pd(OAc)2 and 1-adamantanecarboxylic acid as an additive is the optimized catalytic system, and it yields the corresponding polymer with a molecular weight of 39 400 in 89% yield. The polycondensation reaction, followed by an end-capping reaction, effectively provides a linear polymer without Br terminals." @default.
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• W2012130177 date "2012-10-12" @default.
• W2012130177 modified "2023-10-10" @default.
• W2012130177 title "Detailed Optimization of Polycondensation Reaction via Direct C-H Arylation of Ethylenedioxythiophene" @default.
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• W2012130177 doi "https://doi.org/10.1002/marc.201200550" @default.
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