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- W2012150665 abstract "Niobium(V) in 9 M H2SO4 has been reduced by metallic zinc to a red-brown solution from which a series of salts containing the cluster anion, [Nb6O7(O·SO3)12]16− have been isolated. The compounds have been characterized from analytical, IR spectral and magnetic data and the structure of the cluster and its formation are proposed. The anion is a 12-sulphur trioxide adduct of the ‘Nb6O19’ cluster and contains Nb6(22+) with the average valency of 3.67 for each Nb. Nb6(20+) corresponding to Nb(3.33) and Nb6(26+) corresponding to Nb(4.33) have been potentiometrically shown to be formed as redox derivatives of Nb6(22+) in different aqueous conditions. Isolation of solid Nb(3.33) has been attempted." @default.
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- W2012150665 date "1988-02-01" @default.
- W2012150665 modified "2023-09-24" @default.
- W2012150665 title "SO3 adducts of hexameric oxoniobate cluster in nonintegral subnormal oxidation states: Formation, properties and formulation" @default.
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- W2012150665 doi "https://doi.org/10.1016/s0020-1693(00)80670-2" @default.
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