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- W2012176119 abstract "Abstract New silver(I) derivatives containing bidentate phosphine and anionic bis(triazol-1-yl)borate ligands have been prepared from the reaction of AgNO3 and dppm (bis(diphenylphosphino)methane), dppe (1,2-bis(diphenylphosphino)ethane), or dppf (1,1′-bis(diphenylphosphino)ferrocene) and potassium dihydrobis(1,2,4-triazolyl)borate, K[H2B(tz)2]; their solid state and solution properties have been investigated through analytical and spectroscopic measurements (IR, 1H and 31P NMR). All the compounds are soluble in chlorinated solvents and are non-electrolytes in CH2Cl2 and acetone solutions. [{H2B(tz)2}Ag(dppf)] is simple mononuclear array, the silver atom lying in four-coordinate N2AgP2 environment. In [{H2B(tz)2}2Ag3(dppm)2(NO3)], the silver environment is still four-coordinate but PAgN3, utilizing the coordinating capability of one of the additional (‘exo’-) ring nitrogens not only to complete the four-coordinate array about the silver but, necessarily, to link successive asymmetric units into a single-stranded polymer. [{H2B(tz)2}2Ag3(dppm)2(NO3)] may be regarded as a hemi-adduct of [{H2B(tz)2}Ag(dppm)] with silver(I) nitrate, thus [{H2B(tz)2}Ag(dppm)]: AgNO3 (2:1)." @default.
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- W2012176119 date "2005-01-01" @default.
- W2012176119 modified "2023-10-03" @default.
- W2012176119 title "Silver(I) bis(1,2,4-triazolyl)borate complexes containing bidentate phosphine ligands" @default.
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- W2012176119 doi "https://doi.org/10.1016/j.poly.2004.11.001" @default.
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