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- W2012176128 abstract "Two dinuclear chiral Salen Zn(II) complexes Zn2L (L = N,N′-(1R,2R)(−)-1,2-cyclohexylene-bis(3-hydroxybenzylideneimine)) and Zn2L′(OAc)2 (L′ = N,N′-(1R,2R)(−)-1,2-cyclohexylene-bis(3-methoxybenzylideneimine)) with compartmental, potentially hexadentate Schiff-base ligands L and L′ have been synthesized and characterized by elemental analyses, 1H NMR, mass spectra, UV–Vis spectra and circular dichroism spectra. Their axial coordination with N-containing monodentate ligand (imidazole) and bidentate bridging ligands (ethylenediamine and 1,2-propylenediamine) have been studied by circular dichroism spectral titration, UV–Vis spectral titration and molecular modeling. The results of thermodynamic study, including standard association constants (K θ), and thermodynamic parameters (, , ), together with the energy obtained from molecular modeling suggest that Zn2L can bind two monodentate axial ligands or one bidentate ligand via a bridging mode with its two zinc atoms. However, the complex Zn2L′(OAc)2 can bind two bidentate ligands by a mode that each of its two zinc atoms coordinates to one of the two nitrogen atoms of the bidentate ligand. A small modification on the structure of a complex leads to a distinct binding mode with a certain ligand." @default.
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- W2012176128 date "2007-10-09" @default.
- W2012176128 modified "2023-10-17" @default.
- W2012176128 title "Synthesis, spectral and theoretical studies on axial coordination of dinuclear Salen zinc(II) complexes" @default.
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- W2012176128 doi "https://doi.org/10.1080/00958970701275782" @default.
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