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- W2012180705 abstract "Abstract 2,3:4,5- Di -O- isopropylidene -aldehydo- d -arabinose ( 2 ) was converted by a Wittig reaction into a mixture of ( E/Z)-1- aryl-1,2-dideoxy-3,4:5,6-di -O- isopropylidene- d -arabino- hex-1-enitols ( 4,5 ). Selective deprotection of the 5,6- O -isopropylidene group in compounds 4 and 5 followed by selective silylation at position 6 afforded the separate (Z)-l-aryl -6-O-(tert- butyldimethylsilyl)-1,2-dideoxy -3,4-O- isopropylidene- d -arabino- hex-1-enitols 8a–d and the corresponding E -isomers ( 9a–d ). Iodonium-ion-induced cyclization of compounds 8c and 9a-c furnished stereoselectively the 6-O-(tert- butyldimethylsilyl)-2-deoxy-2-iodo -3,4-O- isopropylidene-β- d -glucopyranosylarenes 10a–c . Full deprotection of compounds 10a–c and the O -acetylation led to compounds 11a–c , which on treatment with tributyltin hydride-azobisisobutyromnitrile yielded and the title compounds ( 12a–c )." @default.
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- W2012180705 title "A method for the synthesis of C-(2-deoxy-β-glycosyl) arenes" @default.
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- W2012180705 doi "https://doi.org/10.1016/0008-6215(95)00321-5" @default.
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