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• W2012200622 endingPage "145" @default.
• W2012200622 startingPage "138" @default.
• W2012200622 abstract "In this study, [Ni(dien)2]⋅smz2⋅(Hsmz: sulfamethazine and dien: diethylenetriamine) complex has been synthesized and its crystal structure has been determined by X-ray diffraction technique. The title complex crystallizes in orthorhombic system with space group Pbnb [a = 8.556(5), b = 16.228(5), c = 28.209(5) Å, V = 3917(3) Å3 and Z = 4]. The nickel(II) ion has distorted octahedral coordination geometry. The metal atom, which rides on a crystallographic center of symmetry, is coordinated by six nitrogen atoms of two dien ligands to form a discrete [Ni(dien)2]2+ unit, which captures two sulfamethazine ions, each through intermolecular hydrogen bonds. The powder EPR spectrum of Cu2+ doped Ni(II) complex was recorded at room temperature. The vibrational investigation has been carried out by considering the characteristic bands related to the functional groups of the complex. The electrochemical behavior of Ni(II) ions in the presence and in the absence of smz and dien were studied by square wave and cyclic voltammetry. A well-defined irreversible peak at −1.112 V different from those of the Ni(II)-smz (−0.876 V) and the Ni(II)-dien complex (−1.064 V) was observed in the solution containing Ni(II) ions, which was attributed to the formation of the new mixed ligand complex of Ni(II) with smz and dien." @default.
• W2012200622 created "2016-06-24" @default.
• W2012200622 creator A5012926051 @default.
• W2012200622 creator A5015921577 @default.
• W2012200622 creator A5090350414 @default.
• W2012200622 date "2015-03-01" @default.
• W2012200622 modified "2023-09-26" @default.
• W2012200622 title "Synthesis, structural and electrochemical properties of nickel(II) sulfamethazine complex with diethylenetriamine ligand" @default.
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• W2012200622 doi "https://doi.org/10.1016/j.saa.2014.10.113" @default.
• W2012200622 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/25485867" @default.
• W2012200622 hasPublicationYear "2015" @default.
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