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• W2012236067 abstract "Electron spin resonance (ESR) spectroscopy was used to characterize the ligand environment of VO2+ absorbed on boehmite and noncrystalline aluminosilicates. Boehmite possessed a relatively low capacity to chemisorb VO2+ at discrete sites at low pH, a fact attributed to the chemical inactivity of the dominant (020) surfaces of the mineral. The chemisorbed cation is rigidly bound by one or two surface oxyanions. Chemisorption on allophane produced slightly different ESR parameters for VO2+, a possible consequence of the participation of silanol groups in the metal-surface bond. Evidence for ternary surface complexes was seen upon the addition of phosphate to the VO2+-surface complexes, with changes occurring in the ESR spectrum of bound VO2+. Oxalate also appeared to perturb the ligand environment of sorbed VO2+, but other anionic species had little or no effect. The experimental results point to the coadsorption of a vanadyl-phosphate complex, in which both the VO2+ and the PO43− are chemisorbed to surface Al atoms. The ESR spectra of VO2+ in model phosphate compounds are used to establish the effect of PO43− coordination with VO2+ on the spectral parameters." @default.
• W2012236067 created "2016-06-24" @default.
• W2012236067 creator A5069034683 @default.
• W2012236067 date "1987-12-01" @default.
• W2012236067 modified "2023-10-17" @default.
• W2012236067 title "Ternary VO2+-ligand-surface complexes on boehmite and noncrystalline aluminosilicates" @default.
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• W2012236067 doi "https://doi.org/10.1016/0021-9797(87)90368-7" @default.
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