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- W2012333268 abstract "4-Hydroxy-2(E)-nonen-1-al-diethylacetal 3 (HNE-DEA) was prepared by condensation of the Grignard compound derived from propiolaldehyde diethylacetal and n-hexanal followed by reduction of the resulting 4-hydroxy-2-nonyn-1-al-diethylacetal 2 with LiAlH4 according to the literature procedure with minor modifications. Swern oxidation [DMSO + (COCl2)] of 3 gave 30% yield of 4-oxo-2(E)-nonen-1-al-diethylacetal 5. [3H]NaBH4 and [2H]NaBH4 reduction of 5 gave rise respectively to [4-3H]HNE-DEA (specific activity 222 GBq/mmol) and [4-2H]HNE-DEA." @default.
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- W2012333268 date "1995-05-01" @default.
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- W2012333268 title "Synthesis of 4-hydroxy[4-3H]-2(E)-nonen-1-al-diethylacetal" @default.
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- W2012333268 doi "https://doi.org/10.1002/jlcr.2580360511" @default.
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