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- W2012336887 abstract "A manometric method for determination of carbon and hydrogen is described which affords significant improvements in accuracy over both previously reported manometric techniques and the conventional Pregl gravimetric method. Water and carbon dioxide from the combustion are collected in dry ice and liquid nitrogen traps, respectively, and selectively vaporized into an evacuated mercury manometer immersed in a bath maintained at a constant elevated temperature. The observed pressure of each component is referred to a calibration curve to determine carbon and hydrogen. Nitrogen oxides are removed by adsorption on activated managanese dioxide in an external scrubber. Une semicro méthode manométrique est décrite pour le dosage du carbone et de l'hydrogène. L'eau et l'anhydride carbonique provenant de la combustion sont recueillis respectivement dans de la glace sèche et dans de l'azote liquide; ils sont ensuite vaporisés dans un manomètre. La précision obtenue est meilleure que celle obtenue avec les méthodes manométriques habituelles ou la méthode gravimétrique de Pregl. Beschreibung einer manometrischen Halbmikromethode zur Bestimmung von Kohlenstoff undWasserstoff. Das bei der Verbrennung gebildete Wasser sowie das Kohlendioxyd werden getrennt ausgefroren und dann selektiv in ein evakuiertes Quecksilbermanometer verdampft. Aus der Druckänderung kann dann der Gehalt an Kohlenstoff und Wasserstoff berechnet bezw. an einer Kalibrationskurve abgelesen werden." @default.
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- W2012336887 date "1960-01-01" @default.
- W2012336887 modified "2023-09-26" @default.
- W2012336887 title "Semimicro manometric method for the determination of carbon and hydrogen in organic compounds" @default.
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- W2012336887 doi "https://doi.org/10.1016/s0003-2670(60)80102-x" @default.
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