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- W2012382303 abstract "Quantitative CO chemisorption measurements were made on nickel catalysts supported on SiO2, Nb2O5 and Nb2O5SiO2 to investigate the nature and stoichiometry of CO adsorption. A close look at conventional methods of performing CO adsorption isotherms revealed that for supported nickel catalysts, the results are quite sensitive to a number of experimental parameters including CO pressure, adsorption temperature and time of equilibration. The formation of Ni(CO)4 was observed even at subambient adsorption temperature. Erroneous adsorption uptakes and unrealistic CONi5 stoichiometries are likely to result if this tendency for carbonyl formation is not recognized and properly taken into account. The extent of carbonyl formation and the effect of the experimental variables just mentioned are support-sensitive. Consequently CO chemisorption data may be used to evaluate the degree of interaction between nickel and the support." @default.
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- W2012382303 title "Carbon monoxide adsorption as a chemical probe of supported nickel catalysts: The role of carbonyl formation and support effects" @default.
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