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- W2012397568 abstract "Bis(triphenylphosphine)iminium Bis(methoxo)phthalocyaninato(2–)ferrate(III) – Synthesis and Crystal Structure Chlorophthalocyaninato(2–)ferrate(III) reacts with bis(triphenylphosphine)iminium hydroxide in methanol/acetone solution to yield blue crystals of bis(triphenylphosphine)iminium bis(methoxo)phthalocyaninato(2–)ferrate(III). The complex salt crystallizes as an acetone/methanol solvate (bPNP)[Fe(OCH3)2pc2–] · (CH3)2CO · 1.5 CH3OH in the triclinic space group P 1 (no. 2) with the cell parameters a = 13.160(5) Å, b = 15.480(5) Å, c = 17.140(5) Å, α = 97.54(5)°, β = 91.79(5)°, γ = 95.44(5)°. The Fe atom is located in the centre of the pc2– ligand coordinating four isoindole N atoms (Niso) of the pc2– ligand and two O atoms of the methoxo ligands in a mutual trans arrangement. The average Fe–O and Fe–Niso distances are 1.887 and 1.943 Å, respectively. The cation adopts the bent conformation (< P–N–P = 140.4(2)°) with P–N distances of 1.579(3) and 1.575(3) Å." @default.
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- W2012397568 date "1998-02-01" @default.
- W2012397568 modified "2023-09-23" @default.
- W2012397568 title "Bis(triphenylphosphin)iminium-bis(methoxo)phthalocyaninato(2-)ferrat(III) - Synthese und Kristallstruktur" @default.
- W2012397568 doi "https://doi.org/10.1002/(sici)1521-3749(199802)624:2<173::aid-zaac173>3.0.co;2-c" @default.
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