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- W2012544908 abstract "In this work, polyvinilydene fluoride (PVDF) microcapsules were prepared by using combined emulsion and phase inversion techniques. With this method, microcapsules with different diameters and porosities have been obtained by just controlling the diameter of the membrane used during the preparation. Using a PVDF solution containing the oxidation catalyst ammonium molybdate (20 wt %), catalytic polymeric microcapsules with diameters ranging from 600 to 1200 μm have been obtained. Characterization of catalytic microcapsules by means of SEM, BSE, and EDX analyses showed a uniform ammonium molybdate dispersion in the polymeric matrix. Catalytic microcapsules have been tested in the oxidation of aromatic primary alcohols to corresponding aldehydes. In the range 600−1200 μm, the microcapsule diameter influences the formation of oxidation products: in particular, microcapsule diameters >900 μm slightly diminish the formation of aldehyde due to a beginning diffusion limitation. An interesting structure−reactivity behavior, induced by the interaction between the polymeric membrane and the substituted aromatic alcohol, has been observed." @default.
- W2012544908 created "2016-06-24" @default.
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- W2012544908 date "2008-08-15" @default.
- W2012544908 modified "2023-09-23" @default.
- W2012544908 title "Combined Emulsion and Phase Inversion Techniques for the Preparation of Catalytic PVDF Microcapsules" @default.
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- W2012544908 doi "https://doi.org/10.1021/jp804897b" @default.
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