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- W2012637605 abstract "A systematic approach was used to evaluate the electrospray ionization mass spectral (ESI-MS) analysis of sucrose octasulfate (SOS), an important pharmaceutical agent. SOS represents a model for other suffated carbohydrates, such as heparin and glycosaminoglycan-derived oligosaccharides that also are highly sulfated and pose difficult analytical problems. A survey of ammonium counterions showed that 1 degree, 2 degrees, and 3 degrees ammonium salts of SOS gave substantial fragmentation as a result of sulfate loss. In contrast, quaternary ammonium and phosphonium salts gave excellent ESI spectra, particularly in the positive ion mode. This represents the first report of the ESI-MS analysis of sulfated carbohydrates in the positive ion mode." @default.
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- W2012637605 date "2003-05-20" @default.
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- W2012637605 title "Evaluation of Counterions for Electrospray Ionization Mass Spectral Analysis of A Highly Sulfated Carbohydrate, Sucrose Octasulfate" @default.
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- W2012637605 doi "https://doi.org/10.1021/ac034053l" @default.
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