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- W2012657291 endingPage "19473" @default.
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- W2012657291 abstract "The efficient and controllable synthesis, the detailed characterization, and the chemical postfunctionalization of polycarboxylated single-walled carbon nanotubes SWCNT(COOH)n are reported. This innovative covalent sidewall functionalization method is characterized by (a) the preservation of the integrity of the entire σ-framework of SWCNTs; (b) the possibility of achieving very high degrees of addition; (c) control of the functionalization degrees by the variation of the reaction conditions (reaction time, ultrasonic treatment, pressure); (d) the identification of conditions for the selective functionalization of semiconducting carbon nanotubes, leaving unfunctionalized metallic tubes behind; (e) the proof that the introduced carboxylic acid functionalities can serve as versatile anchor points for the coupling to functional molecules; and (f) the application of a subsequent thermal degradation step of the functionalized semiconducting tubes leaving behind intact metallic SWCNTs. Functional derivatives have been characterized in detail by means of Raman, UV–vis/nIR, IR, and fluorescence spectroscopy as well as by thermogravimetric analysis combined with mass spectrometry, atomic force microscopy, and zeta-potential measurements." @default.
- W2012657291 created "2016-06-24" @default.
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- W2012657291 date "2011-11-10" @default.
- W2012657291 modified "2023-10-03" @default.
- W2012657291 title "Selective Polycarboxylation of Semiconducting Single-Walled Carbon Nanotubes by Reductive Sidewall Functionalization" @default.
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- W2012657291 doi "https://doi.org/10.1021/ja206818n" @default.
- W2012657291 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/22035086" @default.
- W2012657291 hasPublicationYear "2011" @default.
- W2012657291 type Work @default.